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Nickel Plating (Bright &
Sulfamate)
Typical pH: 4 to 4.5
Temperature: Bright, 140 F (60 C); Sulfamate, 100 to 140 F (38 to
60 C)
Agitation: Moderate to aggressive
In-Tank Filtration: Continuous filtration is imperative to ensure
blemish-free appearance of bright nickel deposits. For electroforming and
other engineering coatings using sulfamate baths, roughness prevention is
top priority.
Carbon Treatment: Frequent or continuous for bright nickel; as
needed for sulfamate.
Pump Material of Construction: CPVC usually specified. Polypropylene
is excellent.
Commonly Used Filter Cartridges: Most customers start with the
FK50 or FK20 Poly-Spun
Disposables or the PMCA or PMCB Permacore Magnum Reusables in the required length.
Depending on the solids generated, it may be desirable to use finer
cartridges (lower micron rating) to remove smaller particles.
Special Notes: If used in a harsh plating environment, the pump must be mounted in a well-ventilated location for maximum motor life. The pump must not be installed in front of the ventilation exhaust, as this will expose the motor to a continuous draft of fumes. In addition, some users brush on the pump motor a thin layer of acid-resistant liquid maskant to prevent perforation corrosion of the motor housing.
Nickel Plating, Woods Strike
Typical pH: less than 1
Temperature: Room temperature
Agitation: Light to moderate
In-Tank Filtration: As needed for
general bath cleanliness.
Carbon Treatment: Rare
Pump Material of Construction: CPVC usually specified. Polypropylene
is excellent.
Commonly Used Filter Cartridges: Most customers start with the
FK50 or FK20 Poly-Spun
Disposables or the PMCA Permacore Magnum Reusables in the required length.
Depending on the solids generated, it may be desirable to use finer
cartridges (lower micron rating) to remove smaller particles.
Special Notes: Because this may be a harsh plating environment, the pump must be mounted in a well-ventilated location for maximum motor life. The pump must not be installed in front of the ventilation exhaust, as this will expose the motor to a continuous draft of fumes. In addition, some users brush on the pump motor a thin layer of acid-resistant liquid maskant to prevent perforation corrosion of the motor housing.
Nickel Plating, Electroless (Autocatalytic)
Typical pH: 4 to 6.5 for nickel-phosphorus (the
most popular type); 10 for the alkaline type
Temperature: 180 to 195 F (82 to 91 C) for nickel-phosphorus; 100
to 150 F (38 to 66 C) for alkaline type
Agitation: Very aggressive for electroless nickel-phosphorus
type (a minimum of 10 turnovers per hour is typical); light to moderate
for alkaline EN bath.
In-Tank Filtration: In-tank filtration frequently provides enough
agitation to replace alternate agitation systems in electroless
nickel-phosphorus baths while providing temperature uniformity and
particulate removal. The alkaline EN baths for plastics plating, aluminum
strikes, and electronics plating (Ni-Boron) may be filtered as needed for
general cleanliness.
Carbon Treatment: Rare, if ever
Pump Material of Construction: Polypropylene is suitable for most applications under 190 F. At higher temperatures, warping may occur. The best material of construction for EN baths is
usually considered to be the high-temperature plastic PVDF (Kynar), but this comes at a premium price
many are unwilling to pa. In very rare cases, stainless steel may be specified.
Commonly Used Filter Cartridges: For in-tank filtration of
electroless plating baths, the most popular strategy is to use fairly
short filter cartridges--10" long (25 cm)--and change them very
frequently. This helps to reduce plate-out on the cartridges
themselves as particulates are captured on the filter fibers. Most EN
platers start with the FK50 or FK20 Poly-Spun Disposables. A smaller number use the PMCA
Permacore Magnum Reusables, but thorough cleaning and neutralization are
essential in order to prevent catastrophic decomposition of the EN
bath. Here is one EN plater's procedure for cleaning the reusable
blankets: (1) At end of each working day, EN solution is transferred from
process tank to holding tank. At this time, operator unrolls Magnum filter
blanket from cartridge core. (2) Operator thoroughly sprays Magnum blanket
with water using hose and spray nozzle or pressure spray washer. (3)
Magnum blanket is placed in EN process tank as it is filled with 50%
nitric acid for tank cleanup. (4) The next day, Magnum blanket is removed
from tank and again thoroughly sprayed with water. (5) Magnum is immersed
in water rinse tank. (6) Magnum is rinsed in a solution containing about
5% ammonia to neutralize any remaining nitric acid. (7) Magnum is
rewrapped around cartridge core, ready for reuse.
Special Notes: The popular EN-phosphorus bath generates a
highly corrosive, fuming, steaming environment. The pump must be mounted in a well-ventilated location for maximum motor life. The pump must not be installed in front of the ventilation exhaust, as this will expose the motor to a continuous draft of fumes. In addition, some users brush on the pump motor a thin layer of acid-resistant liquid maskant to prevent perforation corrosion of the motor housing. Others fashion a hinged tank cover with cutaway (see Bulletin 13.1
in our catalog). The cutaway is large enough to introduce the Flo King
pump body and filter cartridge, but small enough that the motor base and
motor sit on top of the tank cover. Using this arrangement, the motor is
not continuously bombarded by hot, corrosive fumes. Energy conservation is
another benefit, as the tank cover retains bath heat.
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